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Table 6 Aarhus Bay sampling scheme

From: Modern applications for a total sulfur reduction distillation method - what’s old is new again

 

Sample

Container type

Volume (ml)

Treatment

i

Total S

Clear glass vial

1.5

0.25 ml 20% ZnAc

ii

Sulfate concentration

Cryovial

0.5

Flushed with CO2 to remove sulfide

iii

Sulfide concentration

Clear glass vial

1

0.20 ml 20% ZnAc

iv

Thiosulfate and sulfite

Brown glass vial

0.5

Bimane

v

Sulfate/sulfide/‘other’ S isotope composition

N2 flushed 50 ml glass crimp top vial

> 10 ml

2 ml 20% ZnAc